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Extraction method without solvent Options
 
Brennendes Wasser
#1 Posted : 9/24/2023 9:01:07 PM

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When adding the NaOH actually you will get voluminous white clouds of (probably) DMT just at pH 7,5+. I always thought what will happen if I would just try to collect those, but they are probably too fine to ever be filtered. Then if adding more base as you tell it will go dark - while the clouds will also vanish. So I thought DMT will for some weird reason dissolve again at pH > 10.

But that means you can still get some precipitation? Could be a nice thing, as you would not get any risk for emulsions. How does the final product look like - is it very fine dust and therefore you might spill some over, when decanting water?

And probably biggest question what is the yield? Love
 

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ShadedSelf
#2 Posted : 10/11/2023 11:02:21 AM

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Seems like the OP deleted their post?

I decided to give it a go with some Acacia Confusa sample that I had lying around.
After adding NaOH it went dark even before reaching a ph of 10.
Id say the solution gets a bit cloudier, bit its hard to tell, either way it all seems to stay in suspension.

Out of dissapointment I tried adding some NaCl just to see if something could happen, and now there is definitely "stuff" precipitating, I tried adding salt to the acidid solution but that doesnt seem create any sort of precipitation.

I guess now I have to find out wether this stuff is DMT or not.

 
 
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